HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → HCID 22246767, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 2-(3,5-Dichlorophenoxy)ethylamine | HCID 49991 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 22246767 | HCID 22246767 | — |
Reaction Steps
The title compound was prepared from 2-(3,5-dichloro-phenoxy)-ethylamine, Et3N, and methanesulfonyl chloride using the procedure described in Step 2 of Preparation A1. Recrystallization from EtOH provided the title compound. 1HNMR (400 MHz, CDCl3) δ 6.93 (m, 1H), 6.74 (m, 2H), 5.09 (m, 1H), 4.01 (t, 2H), 3.47 (q, 2H), 2.96 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06649657B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-bf22bf37f28a4983a4ef210a183520d5 |
| Source note | uspto-grants-2003_11 |