HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 69544410, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 54063952 | HCID 54063952 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 69544410 | HCID 69544410 | — |
Reaction Steps
A solution of 3-(3-tert-butoxycarbonylamino-propyl)-benzoic acid methyl ester (565 mg) in MeOH (25 mL) was cooled to 0° C. and the solution was saturated with HCl (g). The reaction was stirred at room temperature for 1.5 h and was concentrated in vacuo to provide the title amine (399 mg). MS 194 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06649657B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-b52ee2c5b5424d8a9fcbdedde22264b8 |
| Source note | uspto-grants-2003_11 |