HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22312692, compound → HCID 86584980, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22312692 | HCID 22312692 | — |
| Reactant | HCID 23552772 | HCID 23552772 | — |
| Product | HCID 86584980 | HCID 86584980 | — |
Reaction Steps
Following General Procedure I above using cyclopentyl-α-hydroxyacetic acid (Example P) and 3-(L-alaninyl)-amino-2,4-dioxo-1,5-bis-phenyl-2,3,4,5-tetrahydro-1H-1,5-benzodiazepine hydrochloride (Example 8-W), the title compound was prepared as a white solid (melting point=139-149° C.). Purification was by flash chromatography eluting with CH2Cl2/EtOAc (1:2). Rf=0.50 and 0.39 (CH2Cl2/EtOAc, 1:2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06653303B1 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-a96e01b25da149c7916a0107f0f32e67 |
| Source note | uspto-grants-2003_11 |