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HRID48089

反应详情

EQUATION

反应方程式

HRID 48089 的结构方程式

REACTANTS

反应物

2
结构：O=c1ccn([C@@H]2O[C@H](CO)[C@@H](O)[C@H]2O)c(=O)[nH]1
HCID6029

Uridine

C9H12N2O6

结构：Cc1ccc(C(=O)Cl)cc1
HCID13405

p-Toluoyl chloride

C8H7ClO

PRODUCTS

生成物

1
结构：Cc1ccc(C(=O)OC[C@H]2O[C@@H](n3ccc(=O)[nH]c3=O)[C@H](O)[C@@H]2O)cc1
HCID11588577

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccncc1
溶剂HCID1049

Pyridine

C5H5N

PROCEDURE

实验过程

4-Methylbenzoyl chloride (10 mmol) is added to a solution of uridine (10 mmol) in 20 mL of pyridine. After no further progress occurs as observed by TLC, the volatile components are evaporated in vacuo. The residue is purified using flash chromatography to give the product as a colorless oil.

WORKUP

后处理

  1. customthe volatile components are evaporated in vacuo
  2. customThe residue is purified