Phthalic Anhydride → HCID 11769653, compound

Participants

Reaction Conditions

Reaction Steps

A 100-mL three-necked round-bottom flask was fitted with a reflux condenser and, in a nitrogen atmosphere, the flask was charged with phthalic anhydride (4.0 g, 13.5 mmol) and allyl alcohol (4.58 mL), and the contents were stirred at 90° C. for 30 minutes. The unreacted allyl alcohol fraction was distilled off under reduced pressure to give phthalic acid monoallyl ester (yield 5.66 g).

Provenance & Evidence