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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 481160Generated: October 31, 2026

1-Phenethylamine, (-)- → HCID 69378823, compound

https://huagongshe.com/reaction/481160

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-Phenethylamine, (-)-HCID 75818—
ReactantBenzaldehyde, 4-(phenylmethoxy)-HCID 78109—
Solventtert-Butyl methyl etherHCID 15413—
ProductHCID 69378823HCID 6937882383%

Reaction Steps

0.11 g (0.93 mmol) of (S)-α-methylbenzylamine and 0.26 g (1.23 mmol) of 4-benzyloxybenzaldehyde are mixed in 4 ml of t-butyl methyl ether and stirred for three days at room temperature, and then evaporated under reduced pressure to give a residue, which was then washed with 5 ml of n-hexane, filtered, and dried to give 0.24 (0.77 mmol) of (S)-N-(4-benzyloxybenzylidene)-α-methylbenzylamine (Yield: 83%, purity 90%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06653507B2
Source datasetuspto-grants-2003_11
ORD IDord-9b4f80d3d81e41198dc384fe12ed44c3
Source noteuspto-grants-2003_11