HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Phenethylamine, (-)- → HCID 69378823, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Phenethylamine, (-)- | HCID 75818 | — |
| Reactant | Benzaldehyde, 4-(phenylmethoxy)- | HCID 78109 | — |
| Solvent | tert-Butyl methyl ether | HCID 15413 | — |
| Product | HCID 69378823 | HCID 69378823 | 83% |
Reaction Steps
0.11 g (0.93 mmol) of (S)-α-methylbenzylamine and 0.26 g (1.23 mmol) of 4-benzyloxybenzaldehyde are mixed in 4 ml of t-butyl methyl ether and stirred for three days at room temperature, and then evaporated under reduced pressure to give a residue, which was then washed with 5 ml of n-hexane, filtered, and dried to give 0.24 (0.77 mmol) of (S)-N-(4-benzyloxybenzylidene)-α-methylbenzylamine (Yield: 83%, purity 90%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06653507B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-9b4f80d3d81e41198dc384fe12ed44c3 |
| Source note | uspto-grants-2003_11 |