HCID 86587568, compound → HCID 69971833, compound

Participants

Reaction Steps

To a solution of 84a (141 mg, 0.177 mmol) in 5 mL MeOH, was added 10% Pd-C (50 mg). The mixture was evacuate and flushed with H2 (3×), then was stirred under an atmosphere of H2 for 8 h. The mixture was filtered and concentrated to give 113 mg (quantitative) of 84b. MS (ESI) 638.4 (M+H+), 660.3 (M+Na+), 636.3 (M−H+).

Provenance & Evidence