1,5-Dichloropentane → 1-Thiophen-2-ylcyclohexane carboxylic acid ethyl ester

HRID 481394Notes

Reaction equation

HRID 481394 reaction equation
[CH2:1]([O:3][C:4](=[O:11])[CH2:5][C:6]1[S:7][CH:8]=[CH:9][CH:10]=1)[CH3:2].Cl[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17]Cl>>[CH2:1]([O:3][C:4]([C:5]1([C:6]2[S:7][CH:8]=[CH:9][CH:10]=2)[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13]1)=[O:11])[CH3:2]

Participants

3

Reactant 2

HCID 123531,5-DichloropentaneHCID 93657Ethyl 2-thienylacetate

Product 1

HCID 542284051-Thiophen-2-ylcyclohexane carboxylic acid ethyl ester

Procedure

The dialkylation of (1) was performed as described in Example 1, Step 1 using 1,5-dichloropentane to obtain the title compound (15).

Sources & evidence

ORD record
ord-3cfd553f3f124bec91a1641171f03525
Source dataset
uspto-grants-1998_08
Patent number
US05789415

Reaction notes

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