HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Z-Gln-ome
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | L-Glutamine, N2-[(phenylmethoxy)carbonyl]- | HCID 75855 | — |
| Product | Z-Gln-ome | HCID 7020255 | — |
Reaction Steps
Sulphuryl chloride (1 g) was added to a stirred mixture of N-benzyloxycarbonyl-L-glutamine (100 g) and methanol (1200 ml) and the mixture was stirred at ambient temperature for 24 hours. The mixture was evaporated to give N-benzyloxycarbonyl-L-glutamine methyl ester (105 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05789417 |
| Source dataset | uspto-grants-1998_08 |
| ORD ID | ord-35828f5d2dd941fe9c92d8fa99b1edd2 |
| Source note | uspto-grants-1998_08 |