HRID481487

反应详情

EQUATION

反应方程式

HRID 481487 的结构方程式

PROCEDURE

实验过程

Compound 4 (89 mg, 0.25 mmol) was treated with hydrogen chloride-methanol (5 ml). After the solvent was evaporated in vacuo, the residue (pale yellow solid) was recrystallized from ethanol-diethyl ether to give Compound 5 (91 mg, 85%) as a white solid.

WORKUP

后处理

  1. customAfter the solvent was evaporated in vacuo
  2. customthe residue (pale yellow solid) was recrystallized from ethanol-diethyl ether