HRID481487
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
Compound 4 (89 mg, 0.25 mmol) was treated with hydrogen chloride-methanol (5 ml). After the solvent was evaporated in vacuo, the residue (pale yellow solid) was recrystallized from ethanol-diethyl ether to give Compound 5 (91 mg, 85%) as a white solid.
WORKUP
后处理
- customAfter the solvent was evaporated in vacuo
- customthe residue (pale yellow solid) was recrystallized from ethanol-diethyl ether