Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Piperonylamine → 6,7-dichloro-3-(1,2,3,6-tetrahydropyridin-4-yl)-1H-indole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Piperonylamine | HCID 2723901 | — |
| 반응물 | 6,7-dichloro-1H-indole | HCID 12272802 | — |
| 생성물 | 6,7-dichloro-3-(1,2,3,6-tetrahydropyridin-4-yl)-1H-indole | HCID 18545981 | — |
반응 단계
The title compound was prepared in a fashion similar to that described in Preparation 30 from 6,7-dichloroindole (1.4 g, 7.5 mmol) and 4-piperidone hydrochloride hydrate (2.3 g, 15 mmol). The product was isolated as a white solid. Yield 1.8 g (89%). mp 252°-254° C. FDMS m/e=268 (M+ of free base).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05789402 |
| 출처 데이터셋 | uspto-grants-1998_08 |
| ORD ID | ord-556f79d792834fc8a1b9a9f063f6cf40 |
| 출처 메모 | uspto-grants-1998_08 |