HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 21268313, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-(3-chloropropoxy)-1H-indole | HCID 11694169 | — |
| Reactant | HCID 21268269 | HCID 21268269 | — |
| Product | HCID 21268313 | HCID 21268313 | — |
Reaction Steps
The title compound was prepared in a fashion similar to that described in Example 192 from 6-nitro-3-(1,2,3,6-tetrahydropyridin-4-yl)-1H-indole (0.50 g, 2.1 mmol), 1-chloro-3-(1H-indole-4-oxy)propane (0.43 g, 2.1 mmol) and potassium carbonate (0.32 g, 2.3 mmol). The product was isolated as an orange granular solid. Yield 0.49 g (56%). mp 215°-225° C. FDMS m/e=416 (M+ of free base).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05789402 |
| Source dataset | uspto-grants-1998_08 |
| ORD ID | ord-3363ca198ac646ed83202b4f252e77d4 |
| Source note | uspto-grants-1998_08 |