HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthalonitrile → 1,4-Benzenedimethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthalonitrile | HCID 7042 | — |
| Reactant | 1,4-Cyclohexanedimethanamine | HCID 17354 | — |
| Product | 1,4-Benzenedimethanamine | HCID 68315 | — |
Reaction Steps
It is known to prepare 1,4-bis(aminomethyl)cyclohexane from dicyanobenzene in a two stage process as disclosed, e.g., in DE-A 3,003,730. In the first stage dicyanobenzene is catalytically hydrogenated to produce 1,4-bis(aminomethyl)benzene, which is then catalytically hydrogenated to produce 1,4-bis(aminomethyl)cyclohexane. One disadvantage is that the starting material must be produced with hydrogen cyanide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05789620 |
| Source dataset | uspto-grants-1998_08 |
| ORD ID | ord-df5237de56f24ca5928ad22d0782c545 |
| Source note | uspto-grants-1998_08 |