HuagongsheHuagongshe Chemistry Print Report · For research reference only
(S)-N-(1-phenethyl-pieridin-3-ylmethyl)-N-phenyl-methanesulfonamide → N-(1-phenethyl-pieridin-3-ylmethyl)-N-phenyl-methanesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (S)-N-(1-phenethyl-pieridin-3-ylmethyl)-N-phenyl-methanesulfonamide | HCID 10177321 | — |
| Reactant | HCID 10292684 | HCID 10292684 | — |
| Product | N-(1-phenethyl-pieridin-3-ylmethyl)-N-phenyl-methanesulfonamide | HCID 9799642 | — |
Reaction Steps
The two homogeneous enantiomers (12 and 16) were also obtained by chiral HPLC separation of the racemate 6 (ChiralPak AD column, 10% i-PrOH, 0.1% Et2NH in hexane, 4.7 mL/min, 254 nm): Rt1=13.92 min (16), Rt2=17.02 min (12).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06703383B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-a280e93285f844288841003b35114da2 |
| Source note | uspto-grants-2004_03 |