Toluene → HCID 11325578, compound

HRID 482132Notes

Reaction equation

HRID 482132 reaction equation
[CH2:1]([NH:5][C:6]1[N:11]=[C:10]([NH2:12])[N:9]=[C:8]([NH2:13])[N:7]=1)[CH2:2][CH2:3][CH3:4].N1C(N)=NC(N)=NC=1N.[C:23]1([CH3:29])[CH:28]=[CH:27]C=CC=1>>[CH2:27]([N:13]([CH2:29][CH2:23][CH2:28][CH3:27])[C:8]1[N:7]=[C:6]([NH:5][CH2:1][CH2:2][CH2:3][CH3:4])[N:11]=[C:10]([NH:12][CH2:1][CH2:2][CH2:3][CH3:4])[N:9]=1)[CH2:28][CH2:23][CH3:29]

Participants

4

Reactant 3

HCID 1140TolueneHCID 7955Melamine2×HCID 197831Melamine, butyl- (8CI)

Product 1

HCID 11325578HCID 11325578, compoundYield 4.8%

Procedure

After 1-butanol and water were distilled off from the crude reaction product, toluene was added to the residue. result, 2-n-butylamino-4,6-diamino-1,3,5-triazine in a yield of 4.8% (based on the starting melamine) and 55.5% of the starting melamine were obtained. The toluene solution was analyzed through HPLC. As a result, it was confirmed that a total amount of the other reaction product was extracted.

Workup

  1. distillationAfter 1-butanol and water were distilled off from the crude
  2. customreaction product, toluene
  3. additionwas added to the residue
  4. customresult
  5. customwere obtained
  6. extractionwas extracted

Sources & evidence

ORD record
ord-5a89c4fbc37e49ffab8e5c2bc91c3d32
Source dataset
uspto-grants-1998_08
Patent number
US05792867

Reaction notes

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