HCID 19063418, compound → HCID 19063427, compound

Participants

Reaction Steps

To a solution of 1-(7-benzyloxycarbonylheptanoyloxy)ethyl decyl carbonate (Example 1ac(iv), 4.0 g, 7.9 mmol) in acetic acid (15 ml) was added a catalytic amount of palladium on charcoal (150 mg). The mixture was hydrogenated with H2 at ambient temperature for 5 hours. Acetic acid was removed under reduced pressure. The residue was purified by column chromatography using n-heptane/ethyl acetate (4:1) as eluent.

Provenance & Evidence