HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dichloroethane → Bentazone ammonium
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dichloroethane | HCID 11 | — |
| Reactant | Bentazon | HCID 2328 | — |
| Reactant | Ammonium Carbonate | HCID 517111 | — |
| Solvent | Water | HCID 962 | — |
| Product | Bentazone ammonium | HCID 131720800 | 197.6% |
Reaction Steps
A mixture of 24 g of bentazone (IIa), 4.8 g of ammonium carbonate, 220 g of 1,2-dichloroethane and 300 g of water was stirred at 50°-60° C. for 1 hour. The phases were then separated, and the water was removed under reduced pressure and at 50°-60° C. 25.5 g of bentazone-ammonium were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05795983 |
| Source dataset | uspto-grants-1998_08 |
| ORD ID | ord-7e6e0d864f024637a169f761570a27ce |
| Source note | uspto-grants-1998_08 |