HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 18981065, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Methyl 2-(2-hydroxymethyl-4-ethylphenoxy)propionate | HCID 18981032 | — |
| Catalyst | Pyridine | HCID 1049 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 18981065 | HCID 18981065 | 100.8% |
Reaction Steps
By the method of Example 1, Step H, 26.0 grams (0.109 mole) of methyl 2-(2-hydroxymethyl-4-ethylphenoxy)propionate and 14.3 grams (0.12 mole) of thionyl chloride were reacted in the presence of two drops of pyridine in 120 mL of diethyl ether, yielding 28.21 grams of methyl 2-(2-chloromethyl-4-ethylphenoxy)propionate. The NMR spectrum was consistent with the proposed spectrum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05798316 |
| Source dataset | uspto-grants-1998_08 |
| ORD ID | ord-bb5089597e1f4b77afa17f4fc29a9375 |
| Source note | uspto-grants-1998_08 |