HRID482471

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID69303

m-Tolyl isocyanate

C8H7NO

结构：COc1cc(C)cc(OC)c1C1=NC(N)C(=O)N(C)c2ccccc21

HCID15379622

未命名化合物

PRODUCTS

生成物

结构：COc1cc(C)cc(OC)c1C1=NC(NC(=O)Nc2cccc(C)c2)C(=O)N(C)c2ccccc21

HCID70052504

未命名化合物

收率 94%

PROCEDURE

实验过程

By using 3-amino-1,3-dihydro-5-(2,6-dimethoxy-4-methylphenyl)-1-methyl-1,4-benzodiazepin-2-one as above and by condensing it as above with 3-methylphenyl isocyanate, 1,3-dihydro-5-(2,6-dimethoxy-4-methylphenyl)-1-methyl-3-(3-methylphenylureido)-1,4-benzodiazepin-2-one is obtained; m.p.=260° C.; Yield=94%.