HRID482544

反应详情

EQUATION

反应方程式

HRID 482544 的结构方程式

PROCEDURE

实验过程

The title compound was prepared in a similar manner described in Example 6 starting with allyl isothiocyanate. 4-Allyl-3-hydroxy-5-mercapto-1,2,4-triazole was reacted with 2-bromo-5-nitrothiazole as in Example 6. Crystallization from ethanol and water gave 4-allyl-3-hydroxy-5-[(5-nitrothiazol-2-yl)mercapto]-1,2,4-triazole as a yellow solid.

WORKUP

后处理

  1. customThe title compound was prepared in a similar manner
  2. customCrystallization from ethanol and water