HCID 9803568, compound → HCID 12968239, compound

HRID 48256Notes

Reaction equation

HRID 48256 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[O:10][C:11]3[CH:31]=[C:30]([O:32][CH3:33])[CH:29]=[CH:28][C:12]=3[C:13]=2[C:14]([C:16]2[CH:21]=[CH:20][C:19]([O:22][CH2:23][CH2:24][N:25]([CH3:27])[CH3:26])=[CH:18][CH:17]=2)=[O:15])=[CH:5][CH:4]=1>CO>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[O:10][C:11]3[CH:31]=[C:30]([O:32][CH3:33])[CH:29]=[CH:28][C:12]=3[C:13]=2[CH:14]([C:16]2[CH:21]=[CH:20][C:19]([O:22][CH2:23][CH2:24][N:25]([CH3:27])[CH3:26])=[CH:18][CH:17]=2)[OH:15])=[CH:5][CH:4]=1

Participants

3

Reactant 1

HCID 9803568HCID 9803568, compound

Product 1

HCID 12968239HCID 12968239, compoundYield 68.5%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

1.335 g (3 mmol) of [2-(4-methoxyphenyl)-6-methoxybenzofuran-3-yl][4-[2-dimethylaminoethoxy]phenyl] methanone was reduced to the carbinol by the method described in Example 1. This yielded 920 mg of the title compound as an oil.

Sources & evidence

ORD record
ord-846ea73776144abdab7c5ad6117df1dc
Source dataset
uspto-grants-2004_03
Patent number
US06703407B1

Reaction notes

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