Bromine → HCID 20244870, compound

HRID 482698Notes

Reaction equation

HRID 482698 reaction equation
[ClH:1].Cl.[NH2:3][C:4]1[S:16][C:7]2[CH2:8][CH2:9][N:10]([CH2:13][CH2:14][CH3:15])[CH2:11][CH2:12][C:6]=2[CH:5]=1.[S-:17][C:18]#[N:19].[K+].BrBr>>[ClH:1].[ClH:1].[NH2:19][C:18]1[S:17][C:5]2[C:6]3[CH2:12][CH2:11][N:10]([CH2:13][CH2:14][CH3:15])[CH2:9][CH2:8][C:7]=3[S:16][C:4]=2[N:3]=1

Participants

4

Reactant 3

HCID 24408BromineHCID 516872Potassium thiocyanateHCID 20244892HCID 20244892, compound

Product 1

HCID 20244870HCID 20244870, compound

Procedure

This compound was prepared from 2-amino-6-propyl-5,6,7,8-tetrahydro-4H-thieno[2,3-d]azepine dihydrochloride, potassium thiocyanate and bromine analogous to Example 1.

Sources & evidence

ORD record
ord-d4c9d1c6483d48d7b5cd91fb83ede857
Source dataset
uspto-grants-1986_03
Patent number
US04575504

Reaction notes

Loading…