Bromine → HCID 20244827, compound

HRID 482699Notes

Reaction equation

HRID 482699 reaction equation
[ClH:1].Cl.[NH2:3][C:4]1[S:16][C:7]2[CH2:8][CH2:9][N:10]([CH:13]([CH3:15])[CH3:14])[CH2:11][CH2:12][C:6]=2[CH:5]=1.[S-:17][C:18]#[N:19].[K+].BrBr>>[ClH:1].[ClH:1].[NH2:19][C:18]1[S:17][C:5]2[C:6]3[CH2:12][CH2:11][N:10]([CH:13]([CH3:14])[CH3:15])[CH2:9][CH2:8][C:7]=3[S:16][C:4]=2[N:3]=1

Participants

4

Reactant 3

HCID 24408BromineHCID 516872Potassium thiocyanateHCID 20244824HCID 20244824, compound

Product 1

HCID 20244827HCID 20244827, compound

Procedure

This compound was prepared from 2-amino-5,6,7,8-tetrahydro-6-isopropyl-4H-thieno[2,3-d]azepine dihydrochloride, potassium thiocyanate and bromine analogous to Example 1.

Sources & evidence

ORD record
ord-afce76c586724a9ca596c200bb29ce2c
Source dataset
uspto-grants-1986_03
Patent number
US04575504

Reaction notes

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