HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glyceric acid → Solketal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glyceric acid | HCID 752 | — |
| Reactant | 2,2-Dimethoxypropane | HCID 6495 | — |
| Reactant | L-Glyceric acid | HCID 6326776 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | Solketal | HCID 7528 | — |
Reaction Steps
Alternatively, the 2,3-dihydroxypropanoic acid (D- or L-glyceric acid) is reacted with 2,2-dimethoxypropane without lower alcohol present to prepare 2,3-O-isopropylidene D- or L-glyceric acid which is then reacted with lithium aluminum hydride to produce the solketal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04575558 |
| Source dataset | uspto-grants-1986_03 |
| ORD ID | ord-2a265e764ef74be3891a82215fae5017 |
| Source note | uspto-grants-1986_03 |