HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorobenzaldehyde → 1,3-Dithiolane, 2-(o-chlorophenyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorobenzaldehyde | HCID 6996 | — |
| Reactant | 1,2-Ethanedithiol | HCID 10902 | — |
| Product | 1,3-Dithiolane, 2-(o-chlorophenyl)- | HCID 55015 | — |
Reaction Steps
Following the general procedure described in Example 1, 55.3 gm (0.393 moles) of 2-chlorobenzaldehyde and 37.21 gm (0.395 moles) of 1,2-ethanedithiol gave, after distillation, 65.65 gm (0.303 moles) of a clear, colorless liquid, b.p. 121°-125° C. (0.03 mm/Hg). Elemental analysis for C9H9ClS2 :
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04575565 |
| Source dataset | uspto-grants-1986_03 |
| ORD ID | ord-871905a2d1754f6180de5479986e87a7 |
| Source note | uspto-grants-1986_03 |