HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Naphthaldehyde → 1,3-Dithiolane, 2-(1-naphthalenyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Naphthaldehyde | HCID 6195 | — |
| Reactant | 1,2-Ethanedithiol | HCID 10902 | — |
| Product | 1,3-Dithiolane, 2-(1-naphthalenyl)- | HCID 10868181 | 96% |
Reaction Steps
Following the general procedure as in Example 1, 38.27 gm (0.245 moles) of α-naphthaldehyde and 23.58 gm (0.25 moles) of 1,2-ethanedithiol gave, after evacuating the volatiles, 54.56 gm (0.235 moles) of an orange colored oil (96% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04575565 |
| Source dataset | uspto-grants-1986_03 |
| ORD ID | ord-1513683aee744ec188753c0c2f23074d |
| Source note | uspto-grants-1986_03 |