反应详情

温度

150 °C

Into a 2 liter autoclave is placed 672 grams of the dimethyl ketal of 1-acetyl-3,3-dimethyl cyclohexane prepared according to Example I; 348 grams of allyl alcohol; and 15 grams of sodium acetate. The autoclave is sealed and the contents are heated to 150° C. and maintained at 150° C. for a period of five hours. At the end of the five hour period the autoclave contents are cooled and the autoclave is opened. The resulting product is distilled on a 12" Goodloe column yielding the following fractions:

1. customprepared
2. customThe autoclave is sealed
3. temperaturemaintained at 150° C. for a period of five hours
4. temperatureAt the end of the five hour period the autoclave contents are cooled
5. distillationThe resulting product is distilled on a 12" Goodloe column
6. customyielding the following fractions