Thionyl Chloride → HCID 14273458, compound

HRID 482813Notes

Reaction equation

HRID 482813 reaction equation
[CH2:1]([O:8][C:9]1[CH:14]=[CH:13][C:12]([C:15]2[CH:20]=[CH:19][C:18]([C:21]([OH:23])=O)=[CH:17][CH:16]=2)=[CH:11][CH:10]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7].S(Cl)([Cl:26])=O>>[CH2:1]([O:8][C:9]1[CH:14]=[CH:13][C:12]([C:15]2[CH:20]=[CH:19][C:18]([C:21]([Cl:26])=[O:23])=[CH:17][CH:16]=2)=[CH:11][CH:10]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 44339084'-(Heptyloxy)[1,1'-biphenyl]-4-carboxylic acid

Product 1

HCID 14273458HCID 14273458, compound

Procedure

10 g of 4-n-heptyloxy-4'-biphenylcarboxylic acid and 50 ml of excess thionyl chloride were heated under reflux for 3 hours and thereafter unreacted thionyl chloride was distilled off to obtain 4-heptyloxy-4'-biphenylcarboxylic acid chloride.

Workup

  1. temperatureunder reflux for 3 hours
  2. distillationunreacted thionyl chloride was distilled off

Sources & evidence

ORD record
ord-7282e8d0bc44468088b8f95033a05f19
Source dataset
uspto-grants-1986_03
Patent number
US04576732

Reaction notes

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