HCID 20243469, compound → 4'-(Octyloxy)[1,1'-biphenyl]-4-amine

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Reaction Steps

4'-n-Octyloxy-4-nitrobiphenyl, a known substance, was reduced with hydrogen in an ethyl acetate solution using a Pd/C catalyst and recrystallized from ethanol to obtain 4'-n-octyloxy-4-aminobiphenyl. 3 g of the obtained product was reacted with 2.2 g S-p-(2-methylbutyloxycarbonyl)benzaldehyde in the same manner as described in Example 19 and recrystallized from ethyl acetate to obtain bright yellow crystals.

Provenance & Evidence