HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 53822255, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-Acetoxybenzoyl chloride | HCID 79668 | — |
| Reactant | 3,5-Dimethyl-2,6-octadien-1-ol | HCID 54096015 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 53822255 | HCID 53822255 | — |
Reaction Steps
7 g of 3,5-dimethyl-2,6-octadienol (geraniol) and 6.8 g of triethylamine were dissolved in 50 ml of tetrahydrofuran. 13.4 g of acetylsalicylic acid chloride was added dropwise to the solution under cooling. After stirring at room temperature for 30 minutes, water was added to the reaction mixture and the product was extracted with n-hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04576963 |
| Source dataset | uspto-grants-1986_03 |
| ORD ID | ord-3da29c540ea740139beac75041d13c94 |
| Source note | uspto-grants-1986_03 |