反应详情

温度

100 °C

The glycerol compound (2.7 g) obtained in Example 42 was dissolved in 30 ml of 80% acetic acid, and the solution was heated at 100° C. for an hour. The solvent was then distilled off and the residue was purified by silica gel column chromatography to give 1.3 g of the above-identified compound melting at 48°-49° C.

1. distillationThe solvent was then distilled off
2. customthe residue was purified by silica gel column chromatography