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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 482956Generated: October 27, 2026

Hydrochloric Acid → Sodium 2-(2-hydroxyethyl)amino-5-nitrobenzenesulphinate

https://huagongshe.com/reaction/482956

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantEthanolamineHCID 700—
ReactantBenzenesulfinic acid, 2-chloro-5-nitro-, sodium salt (1:1)HCID 111522—
SolventWaterHCID 962—
ProductSodium 2-(2-hydroxyethyl)amino-5-nitrobenzenesulphinateHCID 20244457—

Reaction Conditions

Temperature100 °C

Reaction Steps

122 g of sodium 2-chloro-5-nitrobenzenesulphinate are kneaded together with 150 g of ethanolamine, and the mixture is gradually heated to 100° C. After 30 minutes at 100° C. 500 ml of water are added, the reaction solution is neutralised with hydrochloric acid, and the sodium 2-(2-hydroxyethyl)amino-5-nitrobenzenesulphinate is isolated as above, by salting out.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04577015
Source datasetuspto-grants-1986_03
ORD IDord-2abea71c554d4ade8c590de5913dfe09
Source noteuspto-grants-1986_03