HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Cyclohexanedicarboxylic acid, 2,5-dioxo-, 1,4-diethyl ester → HCID 13381767, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Cyclohexanedicarboxylic acid, 2,5-dioxo-, 1,4-diethyl ester | HCID 95310 | — |
| Reactant | HCID 178513181 | HCID 178513181 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 13381767 | HCID 13381767 | 123.2% |
Reaction Steps
A mixture of 12.8 g of diethyl 1,4-cyclohexanedione-2,5-dicarboxylate and 13.6 g of aminoguanidine aminoguanidine bicarbonate in 100 ml of n-butanol was heated at reflux for 9 hours. Cooling produced 17 g of the desired intermediate, mdesired intermediate, mp>300° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04577018 |
| Source dataset | uspto-grants-1986_03 |
| ORD ID | ord-0092bcc6b8594dce90c2fd91e034fe90 |
| Source note | uspto-grants-1986_03 |