HRID482970

反应详情

EQUATION

反应方程式

HRID 482970 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

25 g of thiamine hydrochloride (vitamin B1) was dissolved in 50 g of water; to said solution of 25 g of powdery sodium menadione bisulfite was added within about half an hour. After half an hour of agitation, the reaction mass became opalescent and the adduct began to precipitate. After an hour, the precipitate was filtered, washed and dried. 25 g of a white product having the following analysis was obtained.

WORKUP

后处理

  1. additionwas added within about half an hour
  2. waitAfter half an hour of agitation
  3. customto precipitate
  4. waitAfter an hour
  5. filtrationthe precipitate was filtered
  6. washwashed
  7. customdried
  8. customwas obtained