HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Acetate → HCID 908666, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Acetate | HCID 517044 | — |
| Reactant | 3-(Chloromethyl)-6-methoxyquinolin-2(1H)-one | HCID 19003896 | — |
| Solvent | Acetic Anhydride | HCID 7918 | — |
| Product | HCID 908666 | HCID 908666 | — |
Reaction Steps
2.2 Grams of 3-chloromethyl-6-methoxycarbostyril was dissolved in 20 ml of acetic anhydride, then 12 g of potassium acetate was added thereto and stirred at 60°-70° C. for 3 hours. The reaction mixture was poured in an ice-water and the crystals precipitated were collected by filtration. Recrystallized from acetone to obtain 2 g of 3-acetoxymethyl-6-methoxycarbostyril in the form of colorless prism-like crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04578381 |
| Source dataset | uspto-grants-1986_03 |
| ORD ID | ord-696100f73596497c8e266a02eae308cc |
| Source note | uspto-grants-1986_03 |