HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-5-nitrobenzaldehyde → HCID 10482822, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-5-nitrobenzaldehyde | HCID 72933 | — |
| Reactant | Methyl 3-aminocrotonate | HCID 643918 | — |
| Reactant | 3-(N-benzyl-N-methylamino)-2,2-dimethylpropyl acetoacetate | HCID 10108340 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 10482822 | HCID 10482822 | 38.8% |
Reaction Steps
A mixture of 185 mg of 2-chloro-5-nitrobenzaldehyde, 118 mg of methyl 3-aminocrotonate and 292 mg of 3-(N-benzyl-N-methylamino)-2,2-dimethylpropyl acetoacetate in 1 ml ml of 2-propanol was reacted and then purified in the same way as in Example 9 to yield 215 mg of the desired compound (148).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04578395 |
| Source dataset | uspto-grants-1986_03 |
| ORD ID | ord-0c098634fd054a5caeec619339b13de8 |
| Source note | uspto-grants-1986_03 |