HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Nitrobenzaldehyde → HCID 70040181, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Nitrobenzaldehyde | HCID 11101 | — |
| Reactant | Methyl 3-aminocrotonate | HCID 643918 | — |
| Reactant | 3-(N-benzyl-N-methylamino)-2,2-dimethylpropyl acetoacetate | HCID 10108340 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 70040181 | HCID 70040181 | 37.3% |
Reaction Steps
A mixture of 152 mg of 2-nitrobenzaldehyde, 118 mg of methyl 3-aminocrotonate and 292 mg of 3-(N-benzyl-N-methylamino)-2,2-dimethylpropyl acetoacetate in 1 ml of 2-propanol was reacted and then purified in the same way as in Example 9 to yield 195 mg of the desired compound (300).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04578395 |
| Source dataset | uspto-grants-1986_03 |
| ORD ID | ord-dead5250d28f42b1a15877c3d3876551 |
| Source note | uspto-grants-1986_03 |