HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13456443, compound → HCID 11830280, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13456443 | HCID 13456443 | — |
| Reactant | 2,5,5,8-Tetramethylnona-1,6,7-trien-4-one | HCID 13456445 | — |
| Product | HCID 11830280 | HCID 11830280 | — |
Reaction Steps
5.00 g (26.0 mmoles) of 3b were distilled through the same column as used for 3a. The reaction was monitored on GC. The main product 4b was separated by distillation on a good column (Fischer Spalt rohr, 60 theoretical plates) with >97% purity. The yield was 2.55 g (51%). Bp. 68° C./0.2 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04578484 |
| Source dataset | uspto-grants-1986_03 |
| ORD ID | ord-b30bd512f12e4900b052e36c207efc82 |
| Source note | uspto-grants-1986_03 |