HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phloroglucinol → HCID 20243248, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phloroglucinol | HCID 359 | — |
| Reactant | 1-Chloro-3-methyl-2-butene | HCID 10429 | — |
| Product | HCID 20243248 | HCID 20243248 | — |
Reaction Steps
Phloroglucinol was treated with prenylchloride using the same procedure as described in Example 2 to yield prenylphloroglucinol. Prenylphloroglucinol was treated with butyrylchloride, according to the same procedure as described for the preparation of 2,4-dibutyrylphloroglucinol in Example 34 (Method 2) to yield 5,7-dihydroxy-6,8-dibutyryl-2,2-dimethylchroman (36) after chromatography with silica gel (petroleum ether, ethyl acetate, 4:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04578520 |
| Source dataset | uspto-grants-1986_03 |
| ORD ID | ord-eb26de479fe04d759a33a20cb22d36f0 |
| Source note | uspto-grants-1986_03 |