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HRID483312

反应详情

EQUATION

反应方程式

HRID 483312 的结构方程式

REACTANTS

反应物

2
结构：O=S(Cl)Cl
HCID24386

Thionyl chloride

Cl2OS

结构：CCCCCCCCOc1ccccc1C(=O)O
HCID20082775

2-(Octyloxy)benzoic acid

C15H22O3

PRODUCTS

生成物

1
结构：CCCCCCCCOc1ccccc1C(=O)Cl
HCID20311157

2-(Octyloxy)benzoyl chloride

C15H21ClO2

PROCEDURE

实验过程

First, octyloxybenzoic acid was heated in thionyl chloride under reflux until complete dissolution. Excess thionyl chloride was removed by vacuum distillation. Thus there was obtained octyloxybenzoic acid chloride.

WORKUP

后处理

  1. temperatureunder reflux until complete dissolution
  2. customExcess thionyl chloride was removed by vacuum distillation