1,6-Hexanediol → HCID 178459130, compound

HRID 483326Notes

Reaction equation

HRID 483326 reaction equation
[CH3:1][CH:2]([CH3:4])[O-:3].[CH3:5][CH:6]([CH3:8])[O-:7].[CH3:9][CH:10]([CH3:12])[O-:11].[Ti+3:13].O[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20]O>>[CH3:1][CH:2]([CH3:4])[O-:3].[CH3:5][CH:6]([CH3:8])[O-:7].[CH3:9][CH:10]([CH3:12])[O-:11].[OH:3][Ti+3:13][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20]

Participants

3

Reactant 2

HCID 123741,6-HexanediolHCID 9815954titanium(3+) propan-2-olate

Product 1

HCID 178459130HCID 178459130, compoundYield 200%

Procedure

0.1 moles of titanium-tri-isopropoxide (Tyzor TPT DuPont, Wilmington, Del.) and 0.1 moles of 6-hydroxy-1-hexanol were added to a 50 ml beaker and stirred at room temperature for 1 minute to form 0.1 mole of hydroxy-hexyl-titanium-tri-isopropoxide. The reaction mixture was heated to 70 degrees C. for 10 minutes to evaporate the isopropyl alcohol formed during the reaction.

Sources & evidence

ORD record
ord-639a1bb410ff41a98da0e1dece15efa5
Source dataset
uspto-grants-1993_07
Patent number
US05225282

Reaction notes

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