HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 14989466, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 14989464 | HCID 14989464 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14989466 | HCID 14989466 | 83.2% |
Reaction Steps
0.28 g of compound A from Example 1d) in 10 ml of ethanol is stirred with 0.25 g of sodium borohydride for 45 min. Dilution with 1 N NaOH is followed by extraction 2× with EtOAc. Washing of the organic phase with saturated NaCl solution is followed by drying with Na2SO and concentration. 0.22 g of the title compound is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05225414 |
| Source dataset | uspto-grants-1993_07 |
| ORD ID | ord-8eeed7df50874b529fdc8b3823086caf |
| Source note | uspto-grants-1993_07 |