HCID 19752584, compound → HCID 19752511, compound

Participants

Reaction Steps

A mixture of the product from step (b) (257 mg) and 10% Pd/C (110 mg) in ethanol (16 ml) was hydrogenated at room temperature and atmospheric pressure for 6 hours (uptake 12 ml). The mixture was filtered through celite, the residue washed with ethanol and the filtrate evaporated in vacuo to give a colourless oil which was flash chromatographed through a silica column using DCM/ethanol/ammonia (50:8:1 v/v/v) to give the desired product as a colourless oil (87 mg).

Provenance & Evidence