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HRID483416

反应详情

EQUATION

反应方程式

HRID 483416 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)C(C)(C)CC(=O)CSC
HCID15035406

未命名化合物

结构：CC(C)c1ccc(N(N)Cc2ccc(Cl)cc2)cc1.Cl
HCID19752394

1-[(4-Chlorophenyl)methyl]-1-[4-(propan-2-yl)phenyl]hydrazine--hydrogen chloride (1/1)

C16H20Cl2N2

PRODUCTS

生成物

1
结构：CSc1c(CC(C)(C)C(=O)O)n(Cc2ccc(Cl)cc2)c2ccc(C(C)C)cc12
HCID15035388

未命名化合物

PROCEDURE

实验过程

Following the procedure of Example 10, but using 1-(p-chlorobenzyl)-1-[4-(i-propyl)phenyl]hydrazine hydrochloride and methyl 2,2-dimethyl-5-methylthio-4-oxopentanoate as starting materials and hydrolysis at reflux, the title compound was prepared, mp 143°-144°.

WORKUP

后处理

  1. custommaterials and hydrolysis
  2. temperatureat reflux