HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → Benzoyl chloride, 4-(tetradecyloxy)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 4-(Tetradecyloxy)benzoic acid | HCID 289410 | — |
| Catalyst | Chloroform | HCID 6212 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Benzoyl chloride, 4-(tetradecyloxy)- | HCID 9998158 | 102.4% |
Reaction Steps
A mixture of 50 g of p-(tetradecyloxy)benzoic acid and 28.46 g of oxalyl chloride in 500 ml of chloroform containing 10 drops of N,N-dimethylformamide is stirred for 18 hours at ambient temperature. The solvent is evaporated and the residue dissolved in ether, filtered and evaporated to give 54 g of the desired product as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05225425 |
| Source dataset | uspto-grants-1993_07 |
| ORD ID | ord-1525193c99d5448682c4d78a085ff665 |
| Source note | uspto-grants-1993_07 |