反应详情

Scheme Vc, step B: N-{3-[4-(1-Methyl-2-{[(methylethyl)sulfonyl]amino}ethyl)phenyl]propyl}(phenylmethoxy)carboxamide (1 g, 2.31 mmol) and 10% palladium on carbon (0.5 g, 25 mole %) were combined and hydrogenation was carried out in a manner analogous to the procedure described in example 6 to provide the intermediate title compound, {2-[4-(3-aminopropyl)phenyl]propyl}[(methylethyl)sulfonyl]amine, (0.8 g, 87%) as a colorless oil. Electron spray M.S. 299 (M*+H).