HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromopentane → HCID 67638877, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromopentane | HCID 8057 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 67853206 | HCID 67853206 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67638877 | HCID 67638877 | — |
Reaction Steps
was prepared by refluxing 4-(4-hydroxyphenyl)-3-(3,4-methylenedioxyphenoxymethyl)piperidine hydrochloride (0.35 g) with 1-bromopentane (1.8 ml) and K2CO3 (1 g) in abs. ethanol (25 ml) for 2 h. The rinse-up procedure described in example 1 gave the title compound. M.p. 148.2° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05227379 |
| Source dataset | uspto-grants-1993_07 |
| ORD ID | ord-88e5839305a24cdc88e2579df5c4ade1 |
| Source note | uspto-grants-1993_07 |