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HRID483797

反应详情

EQUATION

反应方程式

HRID 483797 的结构方程式

REACTANTS

反应物

2
结构：CCOCCBr
HCID61141

Ethane, 1-bromo-2-ethoxy-

C4H9BrO

结构：N#CC1(c2ccccc2)CCNCC1
HCID181138

4-Piperidinecarbonitrile, 4-phenyl-

C12H14N2

PRODUCTS

生成物

1
结构：CCOCCN1CCC(C#N)(c2ccccc2)CC1
HCID18957813

未命名化合物

PROCEDURE

实验过程

The title compound was prepared as described in Example I 2 from 4-cyano-4-phenylpiperidine and 2-bromoethyl ethyl ether excluding KI: Reaction time under reflux 6 hours. The compound boiled at 130°-135°/0.005 mm Hg.

WORKUP

后处理

  1. customReaction time
  2. temperatureunder reflux 6 hours