Methyl iodide → HCID 22065386, compound

HRID 483852Notes

Reaction equation

HRID 483852 reaction equation
[NH:1]([CH:8]([OH:10])[CH3:9])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH3:11]I>C(O)C>[CH3:11][N:1]([CH:8]([OH:10])[CH3:9])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 4868234HCID 4868234, compound

Product 1

HCID 22065386HCID 22065386, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

In a 250 ml container, take 50 g (0.365 mole) of 2 N anilinoethanol, 52.5 g (0.35 mole) of methyl iodide and 66 ml of ethanol. The solution is left overnight under ethanol reflux.

Workup

  1. temperaturereflux

Sources & evidence

ORD record
ord-591396c993814a2d94a63761596de58b
Source dataset
uspto-grants-1993_07
Patent number
US05227444

Reaction notes

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