m-Anisoyl chloride → HCID 9970412, compound

HRID 483854Notes

Reaction equation

HRID 483854 reaction equation
CO[C:3]1[CH:8]=[CH:7][C:6]([C:9]2[S:10][C:11]3[CH:17]=[C:16]([O:18][CH3:19])[CH:15]=[CH:14][C:12]=3[N:13]=2)=[CH:5][CH:4]=1.[CH3:20][O:21]C1C=C(C=CC=1)C(Cl)=O>>[CH3:20][O:21][C:8]1[CH:7]=[C:6]([C:9]2[S:10][C:11]3[CH:17]=[C:16]([O:18][CH3:19])[CH:15]=[CH:14][C:12]=3[N:13]=2)[CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 74374m-Anisoyl chlorideHCID 10016034HCID 10016034, compound

Product 1

HCID 9970412HCID 9970412, compoundYield 91%

Procedure

The same method as described for 2-(p-methoxyphenyl)-6-methoxybenzothiazole can be used to obtain the corresponding meta isomer by replacing p-methoxybenzoyl chloride with m-methoxybenzoyl chloride. Yield: 91%; melting point: 155°-157° C.

Workup

  1. customto obtain the corresponding meta isomer

Sources & evidence

ORD record
ord-de5a238eac2b43f59ac7fd2edc0a98d3
Source dataset
uspto-grants-1993_07
Patent number
US05227454

Reaction notes

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